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WTC Dust Study Feb 29, 2012 by Dr. James Millette

p.s. I see no date. Inspecting a photo tells me Jan 2014. I'm sure the $5k he's raised could pay for this simple test many times over.

Basile has started by doing completely useless tests that have nothing to do with the original proposal (what they raised the money for). Don't worry though, they say they will keep track of the money spent and anything they don't spend goes to Richard Gage. :rolleyes:

http://www.internationalskeptics.com/forums/showthread.php?t=275738
 
Originally Posted by Miragememories
My hypothesis was that Dr. Millette "likely" performed an unreported 430C heat test to satisfy his own curiosity.

My hypothesis is that Harrit et al "likely" attempted to ignite their samples in an inert atmosphere, as this is such an obvious test it would occur to a 12-year old who has a slight knowledge of the materials in question. They failed, and chose not to publish that fact as it wouldn't suit their purpose.

See how it works, MM?

In my career as an industrial chemist, that's the first thing that would have occurred to me. A simple ignition test under a nitrogen atmosphere would have been the equivalent of dipping litmus or pH paper into a solution to see if it's acid. No pink litmus paper -> no acid. No ignition under nitrogen -> no thermite. Good enough test, though unsophisticated.


Originally Posted by Miragememories
My hypothesis was not unreasonable and I gave a civil explanation for why I thought it probable that Dr. Millette did perform the test referred to.

It was hugely more likely that Harrit et al attempted the 'inert atmosphere ignition' test.

See how it works?

Maybe not. Truthers have repeatedly failed to follow through on obvious lines of investigation, such as interviewing FDNY personnel who supposedly "testified" to hearing suspicious explosions.

The obvious explanation is that deep down, they know that they're wrong, and are afraid to confirm it. So it's quite possible that Harrit didn't do this simple test, not wanting to prove to his own lying eyes that he's wrong.


Originally Posted by carlitos
Again, I am embarrassed to have helped fund this nonsense. As others predicted, it accomplished exactly nothing. Let the truthers wallow in their ignorance. They aren't worth engaging.

I tend to disagree. I noticed a lot of infighting and truthers actually questioning their beliefs as a result of the study. More so than anything else I've seen since 2006. I think it turned a lot of opinions and really hurt the truth movement. Might have been the death nail for relatively sane truthers staying on board.

This is why there was/is such a furious attack on it. It hurt a certain Dick's wallet. I think it was a highly successful study in more than just identifying what was in the dust.

I think you're right, Justin. Trutherism is pretty much down to the hard-core crazies, and "nano-thermite" has pretty much fallen to the wayside.
 
In my career as an industrial chemist, that's the first thing that would have occurred to me. A simple ignition test under a nitrogen atmosphere would have been the equivalent of dipping litmus or pH paper into a solution to see if it's acid. No pink litmus paper -> no acid. No ignition under nitrogen -> no thermite. Good enough test, though unsophisticated.

But......this was super secret stuff and there was air at ground zero. (yes "truther" gurus did point this out early on). No one could know the properties.


:rolleyes:
 
... you're right, Justin. Trutherism is pretty much down to the hard-core crazies, and "nano-thermite" has pretty much fallen to the wayside.
Proof a fringe few failed to gain an education. 911 truth followers can't find evidence when posted, and don't do science. 911 truth movement, a celebration of ignorance.

Real science ignored by faith based 911 truth followers.

The Millette study published, freely on the Internet, 911 truth can't find it.

911 truth's 13th year of failure.
 
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MM once again you completely misrepresent Jim Millette.

I directly confronted him on everything you talk about here.

I asked him what he would do if he found thermite and he said, "If I find it I'll publish it." He also said he is used to presenting results his clients did not like.

Regarding the EPA, he reported dangerous Ph readings and a veritable witches' brew of toxic substances in the dust, which were praised by Cate Jenkins and used as honest measurements in her allegations against the EPA (hear that, Kevin Ryan?). In so doing he also completely contradicted the government claim that the air was safe to breathe a couple weeks after 9/11.

And BTW, he recommended to me people at other labs who could do DSC tests on the chips. He didn't have one in the office, but that would not have stopped him from doing the test if he thought it would be of any value.

He said that he found no thermite in the chips using standard forensic tests, and if the thermitic paper authors wanted to say the chips were incendieries they would have to come up with a new hypothesis about whast these chips are "because they are not thermite."

As for your mockery of my campfire experiment, if YOU had a sincere interest you would like to know if iron-rich microspheres can be found in a regular campfire.

That's the only question I am trying to answer. And again, my hypothesis is that we will not find them there. But we may both be wrong. You are setting the experiment up to be discounted in advance of it even being done, just in case we DO find the microspheres there.

It is not insincerity that keeps me from wasting Millette's time with asking his opinion of Dave Thomas's work.

And I'd really appreciate your revoking the accusation that Millette did a DSC test and didn't report the results. That IS NOT TRUE.

What IS true is that Kevin Ryan's FTIR results and Jeff Farrer's TEM results were not published or released.

You can be soooooo irritating.

You owe us an apology or at least a revocation of that accusation.

On one matter we do agree. I admire the courage of Kevin Ryan, Niels Harrit, Steven Jones, Richard Gage, etc. They have all paid a high price for publicly taking the stands that they have. But that does not make them right. Still, taking a strong stand for what they believe in, is a human attribute that is rare and which I support. Because sometimes people with that kind of courage are right.

"He didn't have one [DSC] in the office his laboratory, but that would not have stopped him from doing the test if he thought it would be of any value."

DR. MILLETTE DID NOT NEED A DSC TO PERFORM A ~430C HEAT TEST!

You know that. It has been pointed out repeatedly here, yet you persist in using it as a fallback argument.

His laboratory is equipped with a muffle furnace which he chose to use in a restricted fashion (he heated samples to 400C instead of ~430C). It is quite adequate for producing testable residue comparable to that highlighted in the 2009 Bentham paper.

The argument made for why he did not use the 430C heat is that it would have destroyed the sample.

It was then pointed out that once he finished collecting data from his 400C-treated samples, he had no scientific argument for not further heating all or some of that material to ~430C.

By your account, Dr. Millette was supposedly looking to retire, yet was supposedly keenly interested in this investigation.
All too conveniently, he became far too busy to publish his work, or spend a few minutes heating up his no longer needed samples for a quick peek under the microscope.

Unlike yourself, I very much doubt Bob Woodward or Carl Bernstein would have been satisfied with such an oddly apathetic response.

The absurdity of your campfire hypothesis is the most desperate red herring I've seen in this thread. It is simply not worthy of more than the briefest of discussion. If you really think it is so worthwhile, why don't you make your own damn campfire instead of asking others to submit their leftovers?

"It is not insincerity that keeps me from wasting Millette's time with asking his opinion of Dave Thomas's work."

Really?

Do you think Dr. Millette is unqualified?

Everyone here opines about the quality and methodology of the work performed by Dr. Harrit et al.

Certainly, I would not expect Dr. Millette to waste his time investigating the quality of Dave Thomas's work.

But, I do believe it would only take him a brief moment to express his opinion about Dave's "trash barrel methodology".

"And I'd really appreciate your revoking the accusation that Millette did a DSC test and didn't report the results. That IS NOT TRUE."

Of course it is not true! I NEVER SAID IT.

A heat test does not equate to only a DSC test. You have made it perfectly clear that Dr. Millette does not possess a DSC.

Because he had the means, a muffle furnace, the no how, the time, and the intense interest, I hypothesized that he "likely" did a further heat test.

If it was an expensive, complex, time consuming test, I could better believe he didn't take a peek.

Regardless, his conclusion that his selected samples were a form of primer paint precludes any match with the highlighted material in the 2009 Bentham paper.

"What IS true is that Kevin Ryan's FTIR results and Jeff Farrer's TEM results were not published or released."

No one said they were published but I have seen a public release of Kevin Ryan's FTIR results. Regarding Dr. Farrer's TEM results being released to the public, I am not sure what you are referring to or how it changes what is already known.

"You owe us an apology or at least a revocation of that accusation."

For the reasons I've given, I still do not owe you an apology or revocation Chris.

It wasn't a lot of my money, but when Dr. Millette accepted it, I and others here became a stakeholders in his still unpublished endeavour.

Promises to test the findings of the 2009 Bentham paper remain broken, and the excuses for not performing the simple 430C heat test are extremely weak.

On Jan.24, 2012, a month before Dr. Millette presented a report on his findings, you posted:

"Here are some things that came up in my most recent conversation with Dr. Jim Millette, who is already well along in his study of the WTC dust:

His [Dr. Millette's] intention is to replicate the tests done in the Bentham study... The Bentham paper does not report on having done a normal environmental forensic study of the components so Dr. Millette will do that, plus everything they did, plus other tests as needed.

And before we re-visit the argument that Dr. Millette did not find proof of unicorns thermite because none was observed, it is very important to note that it has been well argued that Dr. Millette must have worked on similar but different red chips from the many kinds found in the 9/11 WTC dust.

As you know, there are significant differences between the chips Dr. Millette examined and those highlighted in the 2009 Bentham paper.

MILLETTE SAMPLE

- electrical resistivity not measured
- small amounts of titanium found on the surface of a clean slice
- when soaked in MEK for 55 hours the red layer was softened
- when soaked in MEK for 55 hours the red layer did not release any particles
- when heated to 400C and studied, no microspheroids of any kind were found
- when heated to ~430C... results remain unknown as Dr. Millette refused stakeholder requests to perform this simple but critical test, deeming it unnecessary.

"Here, I can agree with you[MM]. Millette can do this simple experiment. Only I doubt that he can really explain expected microspheres in the "ash" in detail (which processes exactly took place), but I can be wrong:cool: This is just my opinion."

BENTHAM SAMPLE

- reference test showed low electrical resistivity
- zero titanium was found on the surface of a clean slice
- when soaked in MEK for 55 hours the red layer did not soften like paint
- when soaked in MEK for 55 hours the red layer showed a significant migration and segregation of aluminum
- some of this aluminum was found to be elemental form
- at 400C no microspheroids have been discovered to exist
- when heated to ~430C and studied, iron-rich microspheroids were found
- when heated to ~430C red chips found to be thermitic ignited with a strong exothermic peak

As a stakeholder in that research performed by Dr. Millette, I feel entitled to challenge his decision to stop short on his testing, especially since he has not published his findings or addressed the discrepancies that exist between the 9/11 WTC dust samples he chose to test and those highlighted in the 2009 Bentham paper.

MM
 
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BENTHAM SAMPLE

- reference test showed low electrical resistivity
- zero titanium was found on the surface of a clean slice
- when soaked in MEK for 55 hours the red layer did not soften like paint
- when soaked in MEK for 55 hours the red layer showed a significant migration and segregation of aluminum
- some of this aluminum was found to be elemental form
- at 400C no microspheroids have been discovered to exist
- when heated to ~430C and studied, iron-rich microspheroids were found
- when heated to ~430C red chips found to be thermitic ignited with a strong exothermic peak
Can you point me to the sample and chip that was run through ALL the tests above? I mean, in order to prove that a chip was thermitic, it needed to yield certain results from ALL the tests above right?

As a stakeholder in that research performed by Dr. Millette, I feel entitled to challenge his decision to stop short on his testing, especially since he has not published his findings or addressed the discrepancies that exist between the 9/11 WTC dust samples he chose to test and those highlighted in the 2009 Bentham paper.

MM
Are you going to get on Harrit's case when he "stopped short" of doing a DSC test and publishing results regarding the Delassio sample?

Are you going to get on Harrit's case when he "stopped short" of doing a resistivity test any of the chips in his possession except for one?

Are you going to get on Harrit's case because he "stopped short" of testing resistivity for paint chips he had in his hands and instead tested paint chips from external sources?

Are you going to get on Harrit's case because he "stopped short" of analyzing the composition of paint chips he had in his hands and instead went to external written compositions?

If all the above tests and their results are important in determining if a chip was thermitic why did he fail to run ALL of them on ALL chips in his paper?
 
MILLETTE SAMPLE

- attracted by a magnet
- electrical resistivity not measured
- small amounts of titanium found on the surface of a clean slice
- when soaked in MEK for 55 hours the red layer was softened
- when soaked in MEK for 55 hours the red layer did not release any particles
- when heated to 400C and studied, no microspheroids of any kind were found
- when heated to ~430C... results remain unknown as Dr. Millette refused stakeholder requests to perform this simple but critical test, deeming it unnecessary.

"Here, I can agree with you [MM]. Millette can do this simple experiment. Only I doubt that he can really explain expected microspheres in the "ash" in detail (which processes exactly took place), but I can be wrong:cool: This is just my opinion."

BENTHAM SAMPLE

- attracted by a magnet
- reference test showed low electrical resistivity
- zero titanium was found on the surface of a clean slice
- when soaked in MEK for 55 hours the red layer did not soften like paint
- when soaked in MEK for 55 hours the red layer showed a significant migration and segregation of aluminum
- some of this aluminum was found to be elemental form
- at 400C no microspheroids have been discovered to exist
- when heated to ~430C and studied, iron-rich microspheroids were found
- when heated to ~430C red chips found to be thermitic ignited with a strong exothermic peak
Can you point me to the sample and chip that was run through ALL the tests above?

I mean, in order to prove that a chip was thermitic, it needed to yield certain results from ALL the tests above right?

Based on my understanding of the contents of the 2009 Bentham paper, a qualifying red chip from the 9/11 WTC dust would;

- have a measured electrical resistance dramatically lower than that of a red primer paint chip from the 9/11 WTC dust
- would have XEDS spectra showing no titanium above the level of noise on the surface of a clean slice
- would not soften when soaked in MEK for 55 hours
- would show a migration and segregation of aluminum after the 55 hour MEK soaking
- would, after MEK soaking for 55 hours show some elemental aluminum
- would produce elemental-iron rich microspheroids when ignited at ~430C
- would produce a strong exothermic peak when ignited at ~430C

Before you start your usual rant about all or nothing, it should be pointed out that NO ONE publishes all their data in a paper.

Scientists publish the amount of data that they and their peers feel is necessary to confirm that paper's findings.

If you can find relevant published papers that contain ALL the data generated, more power to you.

In addition, the scientists, post publication, have stated in public that there were many different red chips. With time and experience they became so familiar with the outward appearance of candidate chips that it was not necessary to apply a regime of tests in order to filter out those that would ignite at ~430C and produce the evidence of thermite.

Dr. Millette lacked that experience which is why people like Dr. Jones wondered why he did not expedite his chip isolation by utilizing the electrical resistivity information published in the Bentham paper.

By only using red chips collected in bulk with a magnet, a method which does allow collection of thermitic red chips, Dr. Millette also collected every red chip that contained magnetically attracted content.

By not bothering to run a 430C heat test in his muffle furnace, Dr. Millette gained no familiarity with the visual differences between red chips that produced a thermitic reaction and those that simply burned to ash (primer paint).

In his unpublished findings, Dr. Millette concluded that his chips must be a formulation of some undetermined steel primer paint.

If steel primer paint behaved in a fashion similar to that observed with the highlighted red chips of the 2009 Bentham paper, Dave Thomas's trash barrel experiment would have been quite the dramatic show!


As a stakeholder in that research performed by Dr. Millette, I feel entitled to challenge his decision to stop short on his testing, especially since he has not published his findings or addressed the discrepancies that exist between the 9/11 WTC dust samples he chose to test and those highlighted in the 2009 Bentham paper.

Are you going to get on Harrit's case when he "stopped short" of doing a DSC test and publishing results regarding the Delassio sample?

Are you going to get on Harrit's case when he "stopped short" of doing a resistivity test any of the chips in his possession except for one?

Are you going to get on Harrit's case because he "stopped short" of testing resistivity for paint chips he had in his hands and instead tested paint chips from external sources?

Are you going to get on Harrit's case because he "stopped short" of analyzing the composition of paint chips he had in his hands and instead went to external written compositions?

If all the above tests and their results are important in determining if a chip was thermitic why did he fail to run ALL of them on ALL chips in his paper?

I believe I have addressed your questions.

It amazes me that you so stubbornly ignore the proof obtained.

Do you not care that hundreds of these thermitic chips have been found?

What possible legitimate reason could thermite have for being there, distributed throughout the 9/11 WTC dust?

Why does it matter whether or not Dr. Harrit et al performed the same tests on every single red chip?
 
Scientists publish the amount of data that they and their peers feel is necessary to confirm that paper's findings.

Wrong. They also need to provide enough data so others can confirm the findings.

Do you believe they provided this in the paper? (so far no one has been able to).

ETA:
- have a measured electrical resistance dramatically lower than that of a red primer paint chip from the 9/11 WTC dust
- would have XEDS spectra showing no titanium above the level of noise on the surface of a clean slice
- would not soften when soaked in MEK for 55 hours
- would show a migration and segregation of aluminum after the 55 hour MEK soaking
- would, after MEK soaking for 55 hours show some elemental aluminum
- would produce elemental-iron rich microspheroids when ignited at ~430C
- would produce a strong exothermic peak when ignited at ~430C

Why is none of this part of the sample separation criteria?
 
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"Scientists publish the amount of data that they and their peers feel is necessary to confirm that paper's findings."
Wrong.

They also need to provide enough data so others can confirm the findings.

Do you believe they provided this in the paper? (so far no one has been able to).

Others being their scientist peers.

What do you believe is lacking from the 2009 Bentham paper that would have made it impossible for Dr. Millette to have duplicated their results?

The paper details what equipment was used and how.

Dr. Millette has his own supply of 9/11 WTC dust.

He has the necessary muffle furnace to ignite the isolated red chips.

He has the facility for performing microscopic examination and XEDS of the created residue.

He was unable to reproduce the results obtained by Dr. Harrit et al because he never attempted to.
 
Others being their scientist peers.

What do you believe is lacking from the 2009 Bentham paper that would have made it impossible for Dr. Millette to have duplicated their results? The paper details what equipment was used and how.

Dr. Millette has his own supply of 9/11 WTC dust.

He has the necessary muffle furnace to ignite the isolated red chips.

He has the facility for performing microscopic examination and XEDS of the created residue.

He was unable to reproduce the results obtained by Dr. Harrit et al because he never attempted to.

The absence of aluminium.
 
What do you believe is lacking from the 2009 Bentham paper that would have made it impossible for Dr. Millette to have duplicated their results?

The poor separation criteria. They specified the method used to separate out the chips. They claim this is all that is needed but according to you, you need to perform all the tests. Why? They did not report any chips using their separation method that were not "thermetic". Poor science.

He was unable to reproduce the results obtained by Dr. Harrit et al because he never attempted to.

He found chips that met the separation criteria. They also matched chemically. Why did they not also report chips separated that were not the same? Poor science.
 
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MILLETTE SAMPLE


- when heated to ~430C... results remain unknown as Dr. Millette refused stakeholder requests to perform this simple but critical test, deeming it unnecessary.

It was unnecessary, and this has been explained to you repeatedly.

This is probably a good place to highlight that what Millette did, was provide an falsifiable test, easily repeatable, that Harrit et al could have checked. See, had the item been thermite, the results of the ashing would have yielded the components that made up thermite, thus proving the sample to contain some kind of thermite substance. It didn't and therefore Millette found no thermite. If Harrit wants to prove Millette wrong, he could repeat the test. But then, Harrit never found aluminum the first time, did he? Think he'll find some the second time around?
 
MM:
It is also likely that the Harrit team knows their conclusions are false. This is why they refuse to share any known "thermite" chips because their bias forbids them from providing the evidence to disprove their claims.

I'm sure glad you clarified the definition of calling someone a liar. ;)
 
Really?

Making a quick perusal I found at least 4 references to a finding of aluminum (Al) in the 2009 Bentham paper.

None of which was found in the post DSC residue, despite your insistence that the DSC residue is what proves it is thermite, and despite the fact that aluminum is a known product of thermite.
 
The absence of aluminium.
Really?

Making a quick perusal I found at least 4 references to a finding of aluminum (Al) in the 2009 Bentham paper.
None of which was found in the post DSC residue, despite your insistence that the DSC residue is what proves it is thermite, and despite the fact that aluminum is a known product of thermite.

Harrit et al said:
"…A conventional quantitative analysis routine was used to estimate the elemental contents.

In the case of this iron-rich spheroid, the iron content exceeds the oxygen content by approximately a factor of two, so substantial elemental iron must be present.

This result was repeated in other iron-rich spheroids in the post-DSC sample as well as in spots in the residue which did not form into spheres.

Spheroids were observed with Fe:O ratios up to approximately 4:1.

Other iron-rich spheres were found in the post-DSC residue which contained iron along with aluminum and oxygen…"

You were saying?
 

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