Money has been raise an tests have begun by independent lab technicians.
Labs have been surveyed for the capabilities they have, including some new capabilities in DSC and Raman (like FTIR).
Staring with known primer chips doing SEM/EDX, FTIR and Raman to characterize chip composition and establish the non production of molten metal/iron from this material during DSC exposure to 400 - 600 Centigrade as well as the exotherm/endotherm character of the primer breakdown.
Next steps: move on to red/gray chips doing the same test, in characterizing composition, then showing the exotherms and reaction products.
Update April 2, 2014
Staring with known primer chips doing SEM/EDX, FTIR and Raman to characterize chip composition and establish the non production of molten metal/iron from this material during DSC exposure to 400 - 600 Centigrade as well as the exotherm/endotherm character of the primer breakdown.
Next steps: move on to red/gray chips doing the same test, in characterizing composition, then showing the exotherms and reaction products.
Proposal:
Sample Preparation:
- Red/gray chip separation using optical microscopy and magnetic attraction to assist in isolation of particles of interest.
- Optical images of collected particulates as collected at appropriate magnifications to record condition as collected.
Sample Analysis:
- SEM/EDX with elemental quantification of red/gray chips, both red and gray layers.
- FTIR analysis of organic components of red/gray chips, both red and gray layers.
- ESCA small spot technique with argon ion sputter for depth profiling to definitively establish the presence of elemental aluminum within the red layer of the red/gray chips. Scans of gray layer also to be taken to add to information base.
- DSC analysis of red/gray chips focusing on exothermic/endothermic reactions near 400 degrees C. Some chips to be scanned in inert atmosphere and some in air or oxygen containing gas stream.
- SEM/EDX with elemental quantification of residual products of DSC analysis of red/gray chips.
- Optical images of reaction products after DSC experiments.
Why are they doing this? This has nothing to do with what they said they were going to do:
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Staring with known primer chips doing SEM/EDX, FTIR and Raman to characterize chip composition and establish the non production of molten metal/iron from this material during DSC exposure to 400 - 600 Centigrade as well as the exotherm/endotherm character of the primer breakdown.
Mark Basile said:Purpose: to see if the following study can be replicated.
Repeatable experiments is fundamental to the scientific method.
Any updates on when they plan to start? They've had the money for a while. The only thing I've seen is the plan of what to do with the money they don't spend (give it to Gage).
Does anyone actually think they will do the study as planed?
Is it a prerequisite for asking about the study?Yes I do.
Are you a stakeholder in the research?
Is it a prerequisite for asking about the study?
Why have they started by wasting money on tests that have nothing to do with the original study? Do they have tons of money to burn?
"Hey, if the "Stakeholders" don't hold their feet to the fire, just like with the earlier flawed study byHarritMillette..."
Fixed that for ya.
Fixed that for ya.
Did the test any of the chips they found not to be "thermetic"? It would appear not because the copied the "paint chip" data out of a book.Are you saying there are no flaws with the Harris study? Tell me, what sample size should they have used? Did they use any known thermite samples for comparison?
Are you saying there are no flaws with the Harris study? Tell me, what sample size should they have used? Did they use any known thermite samples for comparison?