• Quick note - the problem with Youtube videos not embedding on the forum appears to have been fixed, thanks to ZiprHead. If you do still see problems let me know.

WTC Dust Study Feb 29, 2012 by Dr. James Millette

"Of course in the Bentham paper, the value of the observations was not so much about the temperature at which the curve spiked.

Knowing that ignition occurred around 430C was certainly useful, but the intensity and brief duration of the spike was a behavior that made those 9/11 WTC dust chips 'stand out from the crowd'.

The strong thermitic evidence provided by the ignited chips' iron-rich microsphere residue has not been reported anywhere as an expected consequence of heating primer paint of any formulation to those temperatures and much higher."

Unfortunately just about everyone here would rather skirt around any evidence that fails to support their frozen belief.

". . .Besides them saying so, what is the evidence? :confused:"

The 'them', are accredited scientists with long careers in advanced research and have published many peer-reviewed papers.

DGM repeats his baseless claim that there is no evidence of thermitic material in the 9/11 WTC dust.

But unless he is deliberately lying, or over confident in his knowledge, DGM should have valid proof that the Bentham paper evidence finding the existence of thermitic material in the 9/11 WTC dust is wrong? Please explain how their proof has been misinterpreted?

Dr. Millette, a man very familiar with 9/11 WTC dust, having explored it for the government; in his unpublished paper 'skirted' debunking the Bentham paper by 'minimizing' how closely he followed it.

He minimized to the point that the comparability of his isolated and selected samples to those of the Bentham paper scientists was also very minimal.

Then Oystein enters the fray.

He has a good mind so maybe he will address my concerns with some possible alternative explanations?

"
  • Is this why you demand that some tests be done to precisely 430 °C?
    Can you detail the why and how knowing this is value useful? For example, what difference does this make vs. a spike at, say, 480 °C, or 380 °C?
    Can you cite anything that shows that "The strong thermitic evidence provided by the ignited chips' iron-rich microsphere residue has been reported anywhere as an expected consequence of heating nanothermite of any formulation to those temperatures and much higher"?
    For example, do you have any reports of nanothermite igniting/peaking near 430 °C like the red-gray chips did?
    Do you have any reports of nanothermite burning at peak values of 10-24 W/g in a DSC experiment like the red-gray chips did?
    Do you have any reports of nanothermite giving off 4.5 or 7.5 kJ/g like two of the red-gray chips did?
    Do you have any reports of nanothermite residue still having lots of red iron oxide left over visibly after the reaction, as shown in Fig. 20, 23 and 26 of the Bentham paper?
"

Unfortunately, Oystein prefers skirting and misinforming as well.

I asked that Dr. Millette, who only tested his samples to 400C, test proper samples (remove any that had high resistance readings as would steel primer paint), and take his oven as high as 450C.

My understanding is that most of the red chips ignited around 430C.

As Oystein knows, and the Bentham paper clearly states, the temperature of 430C was approximate and not precise for individually ignited chips.

The rest is a barrage of previously addressed points that represents additional skirting of my original post.

He ignores the smoking gun.

Where none existed prior to ignition, iron-rich microspheres existed afterwards in the 9/11 WTC dust chip residue.

Proof of an iron-melting temperature.

What question eliminates that finding?

Next.

". . .
As a retired industrial chemist, I can assure truthers that chemists would be very interested in a result like this.

Could paint resins be undergoing some kind of heretofore unknown exotic reaction, perhaps akin to peroxide formation in ethers? We'd want to know! I guarantee you that others would do follow-up experiments! (I've seen some odd reactions in my own career.)

OK, back to reality: This will never happen, as Jones and Harrit are charlatans. They know damn well what their results will be. The null hypothesis will be supported - it's paint.

Truthers, you've been played. You've been punked. It's your own fault. Even if you're ignorant of chemistry, you swallowed their bunkum and never bothered to solicit the opinions of knowledgeable people in the field of analytical chemistry.
"

You totally lose when without any justification you address distinguished scientists such as Dr. Jones and Dr. Harrit as "charlatans".

Next.

"MM ignored the last 100 pages of thermite threads and still going on about "higher peak = better thermite" fallacy?

And yes, thanks Ivan, that is what I was looking for. So suffice to say, short of finding a paint chip from WTC and burning it, these are the best we have so far for comparing the Bentham DSC of "thermite"?
"

No, you are ignoring the thermitic residue.

Next.

"Excellent post Redwood. As a non-chemist I had no choice but to ask for feedback re the Jones/Harrit paper. Even I can understand, with help, many of the objections raised by this paper. And you are right that chemists would find such a paper as you suggested VERY interesting. Millette himself was VERY interested in what he would find before he found it, and he got a LOT of interest from forensic scientists at two conventions where he made his public presentations about the WTC dust. There is a lot of interest in all forensic questions re 9/11, and an unexplained legitimate strong exothermic reaction w/o oxygen would indeed be powerful stuff!"

Yes, "Millette himself was VERY interested".

Yes, so interested, that even though he has access to 9/11 WTC dust and owns his own lab, he wasn't curious enough to use the Bentham paper simple Resistivity test to further match his samples, and he was unwilling to observe the effect of heating his oven a further 30C-50C from the 400C he stopped at.

Classic skirting as previously noted.

Next.

"One thing that has struck me when I read this study for the first time and when I re-read it again yesterday is the attempt to dissolve the "epoxy resin" with various solvents over various lengths of time. The really couldn't dislodge the red layer, no matter how strong the solvent was or how long the chips were in the solvent. Maybe they couldn't dissolve the red layer because it wasn't epoxy resin. Techniques that are normally used to dissolve expoxy resin should dissolve expoxy resin.

Overall this paper suffers from the same problem as almost every other paper written from about the WTC dust. There's no attempt at context. There is no explanation for the existence of these iron fragments. I understand that this was a narrow paper, meant only to address the issue of thermite. Not finding thermite was a reasonable result.

But from a scientific point of view, this paper doesn't break new ground. The thermite theory was very weak from the beginning. The thermite hypothesis debunks itself. What is missing from the paper is something along the lines of "We started out with tall steel buildings and ended up with iron fragments. Here's why this happened."

Finally, the paper pre-isolates magnetic portions of the dust, and tests those. It doesn't test the other components.
"

This scientific paper wants the reader to seek the context.

The Bentham paper represents the peer-reviewed work of scientists with many years of experience.

Those scientists tested 9/11 WTC dust samples from 4 separate NYC locations near the WTC.

They found similar evidence of thermitic material in all the samples.

Thermitic material, and especially nano-thermitic material, should not have existed anywhere outside of a U.S. military site or some other government-sanctioned facility. For it to permeate all the 9/11 WTC dust, at the very least means there was too much at that location to be explained away as a travelling sample.

The context created by a finding of nano-thermite gets quite clear when you have so much of this special military-grade munition stored in a civilian office tower.

Next.

"Hi WTCDust, What you read in Millette's preliminary study is his answer to the question I hired him to research: is there thermitic material in the red-grey chips from WTC dust as claimed by Jones/Harrit et al? His answer was no. He pre-isolated the red-grey chips to test using the same criteria as described in the Harrit/Jones paper. He charged us $1000 for work that would have been 6 to 10 times more expensive just for these specific red-grey chips. . ."

Yes, Dr. Millette's answer to the question.

An answer based on the question as Dr. Millette chose to interpret it.

For many, such as myself, we contributed to the $1,000 because we felt an honest attempt by a reputable scientist was going to be made to replicate the findings of the Bentham paper scientists.

It was only after we spent our money that it became clear that the money was subsidizing a convention paper that Dr. Millette was already working on, and, that he would not be conducting any of the tests that lead to the key findings published in the 2009 Bentham paper.

Pity.

MM
 
DGM repeats his baseless claim that there is no evidence of thermitic material in the 9/11 WTC dust.

But unless he is deliberately lying, or over confident in his knowledge, DGM should have valid proof that the Bentham paper evidence finding the existence of thermitic material in the 9/11 WTC dust is wrong? Please explain how their proof has been misinterpreted?



MM

The old reverse burden of proof. Funny how your heroes paper has gained zero traction.

I don't have to explain it. Their data did it for me. :rolleyes:
 
Last edited:
I asked that Dr. Millette, who only tested his samples to 400C, test proper samples (remove any that had high resistance readings as would steel primer paint), and take his oven as high as 450C.
Millette did not test any of his chips at this temperature. You have been told at least a dozen times why Millette heated his samples to 400°C, even Millette tells you, however, being the dishonest truther you are, you wilfully ignore this reason over and over.

I shall tell you once more even though I doubt it will penetrate your robust cranium!

The reason why Millette heated his chips to 400°C was to remove the epoxy from paint so he could then further study the particles that were freed. Millette states why he uses low temperature ashing. There is absolutely no point in heating a sample when you already know what the material is due to performing low temperature ashing and TEM-SAED on the particles.

Millette heating his chips has absolutely nothing to do with DSC or micro-spheres or the thermite reaction. Millette heating his chips has no connection with any heating in the Harrit et al paper.

My understanding is that most of the red chips ignited around 430C.

As Oystein knows, and the Bentham paper clearly states, the temperature of 430C was approximate and not precise for individually ignited chips.
So what? This has nothing to do with Millette's reason for heating his chips. You are falsely equating the two. Stop it.

Until you can grow up and accept this truth rather than wilfully ignoring the reason there is no point in engaging with you on any of your other frivolous questions.

You probably have me on ignore because you can't handle my posts.

MM- are samples a-d in Harrit et all the same material? You have yet to agree with everyone including me, Millette, Harrit, Basile and Jones on this point? Why will you not agree?
 
Ya got punked.

The 'them', are accredited scientists with long careers in advanced research and have published many peer-reviewed papers.

Neither Harrit nor Jones have any expertise in analytical chemistry, as evidenced by their paper. Jones' reputation even before his foray into Trutherism was less than sterling - n.b. the cold fusion fiasco.

Dr. Millette, a man very familiar with 9/11 WTC dust, having explored it for the government; in his unpublished paper 'skirted' debunking the Bentham paper by 'minimizing' how closely he followed it.

The Bentham paper is a hopeless hash even if you charitably credit it with being sincere research. They don't specify their procedures and protocols.

Yes, "Millette himself was VERY interested".

Yes, so interested, that even though he has access to 9/11 WTC dust and owns his own lab, he wasn't curious enough to use the Bentham paper simple Resistivity test to further match his samples, and he was unwilling to observe the effect of heating his oven a further 30C-50C from the 400C he stopped at.

This being an example. Briefly explain the role of a resistivity test in a test for thermite.

The Bentham paper represents the peer-reviewed work of scientists with many years of experience.

You said that already. See above.

For many, such as myself, we contributed to the $1,000 because we felt an honest attempt by a reputable scientist was going to be made to replicate the findings of the Bentham paper scientists.

In science, you don't set out to replicate the findings of others. You do your own independent analysis using sound procedures, as Dr. Millette has done.

It was only after we spent our money that it became clear that the money was subsidizing a convention paper that Dr. Millette was already working on, and, that he would not be conducting any of the tests that lead to the key findings published in the 2009 Bentham paper.

The term is "conference paper". Conference papers are easier to get presented than peer-reviewed papers. One purpose of conference papers is to get feedback from other scientists. Maybe Jones and Harrit could do a conference paper on their research, and present their infrared spectroscopy data and x-ray diffraction data, along with a DSC done under an inert atmosphere.

If you and they are right, and this is thermite, it will yield a strong exotherm under an inert atmosphere. Chemists everywhere will want to know how something that looks like common paint reacts like that! I can guarantee that the chemists at Pittsburgh Paint, Sherwin-Williams, et al will be hard at work examining these chips. If you, Harrit, and Jones are correct, then out of pure self-interest, these chemists be publishing papers demonstrating that it's not paint at all, but :eek:military-grade nanothermite:eek: diabolically disguised as paint!

Ain't gonna happen of course. Jones and Harrit are charlatans and will never do this. They know damn well it's paint, and they're not stupid enough to try and fake their results, and don't have the capability to concoct an actual thermite with metallic aluminum platelets that resemble kaolinite. You Truthers got punked. And it's your own fault.
 
...
Unfortunately, Oystein prefers skirting and misinforming as well.
...

The only one skirting anything is YOU, MM. You quote my questions only to dodge them:

Can you cite anything that shows that "The strong thermitic evidence provided by the ignited chips' iron-rich microsphere residue has been reported anywhere as an expected consequence of heating nanothermite of any formulation to those temperatures and much higher"?
  1. For example, do you have any reports of nanothermite igniting/peaking near 430 °C like the red-gray chips did?
  2. Do you have any reports of nanothermite burning at peak values of 10-24 W/g in a DSC experiment like the red-gray chips did?
  3. Do you have any reports of nanothermite giving off 4.5 or 7.5 kJ/g like two of the red-gray chips did?
  4. Do you have any reports of nanothermite residue still having lots of red iron oxide left over visibly after the reaction, as shown in Fig. 20, 23 and 26 of the Bentham paper?
That's four (4) questions.

If you don't answer these four (4) questions properly (either with "no", or with "yes"+citation), you are, as usual , a coward.

If you answer them any different from "no", "no", "no", and "no", respectively, you are a liar.


Please answer the four questions to your best ability!
 
Please do NOT derail this thread with nonsense stuff about toilets! You will be reported if you try again. Thanks for your cooperation.

In the meantime, please acknowldge posts 2672 and 2673, which challenge your FALSE assertion that epoxy will dissolve in the solvants that Millette tried, and ask you to provide evidence in case you don't accept the refutation lashed against you by an eminant scholar in the relevant field of polymer chemistry!

OK, but why did they try it if the technique generally doesn't work for epoxy resin? Millette is the one who tried to dissolve the epoxy resin. Millette is the one who failed to dissolve the epoxy resin. Millette is the one who reported that the attempt to dissolve the epoxy resin was not successful. He didn't have to do all that. He didn't have to attempt to dissolve the resin, but he did. I wonder why?

The kaolin point is important. If kaolin was found (and it appears to have been found), that is data ! We can't throw it out.
 
OK, but why did they try it if the technique generally doesn't work for epoxy resin? Millette is the one who tried to dissolve the epoxy resin. Millette is the one who failed to dissolve the epoxy resin. Millette is the one who reported that the attempt to dissolve the epoxy resin was not successful. He didn't have to do all that. He didn't have to attempt to dissolve the resin, but he did. I wonder why?
Hold it, please: Millette did not say he expected epoxy to dissolve! YOU said so:
Techniques that are normally used to dissolve expoxy resin should dissolve expoxy resin.
the red layer didn't behave like epoxy resin when they tried to dissolve it. This is curious. This indicates that it might not be epoxy resin (because it didn't dissolve like epoxy resin would be expected to dissolve).
Can you please acknowledge first that YOU made an unsupported claim there, and retract it?
I don't see what Millette did wrong.

In fact, it seems that he DID get the expected result for epoxy, so the solvent tests corroborate, or are consistent with, the finding that these red layers are indeed epoxy-based. Do you agree with this?



The kaolin point is important. If kaolin was found (and it appears to have been found), that is data ! We can't throw it out.
Of course kaolin is important. Toilets and their state after the collapses are not, even if they contain kaolin. Please stay on topic.
 
........

Kaolin is also a major component of toilets and sinks, just to add that point. Kaolin is the major component of porcelain. There were no intact toilets or sinks found in the debris. Hmmmm.
......
The main reason the Twin Towers were empty and scheduled for demolition was those hideous steel lined epoxy coated red porcelain toilets and sinks.
 
Last edited:
Hold it, please: Millette did not say he expected epoxy to dissolve! YOU said so:


Can you please acknowledge first that YOU made an unsupported claim there, and retract it?
I don't see what Millette did wrong.

In fact, it seems that he DID get the expected result for epoxy, so the solvent tests corroborate, or are consistent with, the finding that these red layers are indeed epoxy-based. Do you agree with this?




Of course kaolin is important. Toilets and their state after the collapses are not, even if they contain kaolin. Please stay on topic.

Millette was the one who attempted to dissolve the epoxy resin. He did this for some reason. Perhaps he thought it might succeed. It did not succeed, but the fact that he tried using all these solvents with various incubation conditions cannot be ignored.

The failure to dissolve the epoxy resin is at least one hint that the red layer wasn't epoxy resin. The failure of the red layer to dissolve is not proof positive that it was epoxy resin.

If you do a short google search, you will find that regular people encounter epoxy resin and dissolve it with ... heat and organic solvents ... just like Millette tried to do. Epoxy resin can be dissolved with heat and organic solvents. The failure for the red layer to dissolve (even with extended periods of heat, organic solvents, and stirring) means that it might not be epoxy.

Solvents and heat dissolve epoxy. Period. The red layer didn't dissolve with extended solvent and heat treatment. Millette said it. Can't take it back.
 
...
Solvents and heat dissolve epoxy. Period. The red layer didn't dissolve with extended solvent and heat treatment. Millette said it. Can't take it back.
Which solvent, and what temperature. wait, is this like your beam weapon you can't technically specify or identify?

Solvents don't dissolve epoxy (you forgot to specify what solvents, temperature and time). That is a general statement, which is false. You need to specify the epoxy, the solvent, and the temperate, and time of exposure.

...
Where none existed prior to ignition, iron-rich microspheres existed afterwards in the 9/11 WTC dust chip residue.

Proof of an iron-melting temperature.


MM
What?

What temperature is that? Go ahead, be specific; what temperate was reached when the dust burned.

You have proof that iron-rich micro-spheres are found when things burn, as verified by things that burn. The lack of knowledge that iron spheres happen in fires, is making it easy for you to fall for fraud.
 
Last edited:
Millette was the one who attempted to dissolve the epoxy resin. He did this for some reason. Perhaps he thought it might succeed. It did not succeed, but the fact that he tried using all these solvents with various incubation conditions cannot be ignored.

The failure to dissolve the epoxy resin is at least one hint that the red layer wasn't epoxy resin. The failure of the red layer to dissolve is not proof positive that it was epoxy resin.

If you do a short google search, you will find that regular people encounter epoxy resin and dissolve it with ... heat and organic solvents ... just like Millette tried to do. Epoxy resin can be dissolved with heat and organic solvents. The failure for the red layer to dissolve (even with extended periods of heat, organic solvents, and stirring) means that it might not be epoxy.

Solvents and heat dissolve epoxy. Period. The red layer didn't dissolve with extended solvent and heat treatment. Millette said it. Can't take it back.
Then how do you account for the FTIR trace? You are going down the line of a typical truther; you concentrate on an ambiguous test and completely ignore the FTIR testing and data that proves conclusively that the material IS epoxy. I notice you haven't got back to us with your analysis of the FTIR data yet.

The reason why Millette looked to use solvents to dissolve the carbon based (epoxy) matrix was because this method was used in the Harrit et al paper, namely with MEK. If you had read the papers you'd know this. Secondly Millette is trying to free the particles (pigments) that are embedded in this epoxy so that he can perform further, definitive testing in order to characterise them, which he succeeds in doing. Because the epoxy didn't dissolve, which isn't surprising, he had to use another technique, which is why he used low temperature ashing. Again if you had read his progress report carefully and understood the methodology you would know this.
 
MM, WTC Dust:

A few quick comments on a busy morning.

WTC Dust my apologies for thinking you were part of the mininukes crowd. I haven't taken the tuime to study what your hypothesis is, to save me time can you tell me briefly? My main point remains though: WHATEVER your hypothesis, do as I did and try to find a reputable scientist who can test it. What I see now is a hunt for anomalies, which is fine.

MM as you well know, neither you nor I are qualified to make scientific proclamations. However, I at least am making an hopnest effort to try to organize ways to test the various 9/11 Truth hypotheses. You have repeatedly complained about how you wasted your money in contributing to the Millette experiments. Please do one of two things: either ask me for your money back, which I will cheerfully refund with interest immediately upon request, or quit complaining about the money you spent. It's passive-aggressive and irritating.

As for accusations that I am skirting the issues, I am not qualified to rebut or agree with claims that Millette got the wrong chips or didn't heat the chips enough. I am attempting to organize another test, however. Someone has agreed (when he has time) to find known primer paint on steel, heat it to 700 degrees C or more, then look to see if he can find any iron-rich microspheres that were created by such a fire (at regular sub-steel-melting temps). As for the resistivity and soft/hard layer issues, as far as I can see they were never listed in the Jones/Harrit paper as part of their protocol for separating out the red-grey chips. Millette appears to me to have followed the Jones/Harrit protocol to the letter as far as separating out the chips. And keep in mind that my request for chips Jones/Harrit considered to be thermitic were angrily rebuffed by Kevin Ryan. All problems relat8uing to the issue of Millette and the "wrong chips" could be instantly solved through cooperation among the parties, which at this time is nonexistent. I am working on this as well and am fashioning a letter requesting again samples of their chips for experimentation. It's extremely frustrating to ask for chip samples, be angrily rebuffed, and then have Jones claim Millette found the wrong chips!
 
All problems relat8uing to the issue of Millette and the "wrong chips" could be instantly solved through cooperation among the parties, which at this time is nonexistent. I am working on this as well and am fashioning a letter requesting again samples of their chips for experimentation. It's extremely frustrating to ask for chip samples, be angrily rebuffed, and then have Jones claim Millette found the wrong chips!

will millette give some chips to interested parties?
 
Interesting Harrit/Jones wouldn't do this. Strange "truthers" don't question this (or even think to demand it). :rolleyes:
To their credit, several 9/11 Truth activists agree with me that Jones/Harrit/Ryan should release samples of their chips to Millette. One of them even called Kevin Ryan's behavior "childish."
 
To their credit, several 9/11 Truth activists agree with me that Jones/Harrit/Ryan should release samples of their chips to Millette. One of them even called Kevin Ryan's behavior "childish."
Agreeing with you and seeing it as they are hiding something are two worlds apart. I'm sure you see the hypocrisy. Could you imagine the number of YouTube videos (the true measure of "truther" importance) if the roles were reversed?
 
Millette was the one who attempted to dissolve the epoxy resin. He did this for some reason. Perhaps he thought it might succeed. It did not succeed, but the fact that he tried using all these solvents with various incubation conditions cannot be ignored.

Hold it, please: Millette did not say he expected epoxy to dissolve! YOU said so:

The failure to dissolve the epoxy resin is at least one hint that the red layer wasn't epoxy resin. The failure of the red layer to dissolve is not proof positive that it was epoxy resin.

See, YOU make that unsupported claim again!

If you do a short google search, you will find...
Link and quote, please!

that regular people encounter epoxy resin and dissolve it with ... heat and organic solvents ... just like Millette tried to do.
MUUUUP
Millette did NOT use heat AND organic solvents. He used organic solvents ONLY, and, in different tests, heat ONLY to free the pigments from the epoxy.

Epoxy resin can be dissolved with heat and organic solvents. The failure for the red layer to dissolve (even with extended periods of heat, organic solvents, and stirring) means that it might not be epoxy.
Again, Millette did NOT use heat AND organic solvents.

Solvents and heat dissolve epoxy. Period. The red layer didn't dissolve with extended solvent and heat treatment. Millette said it. Can't take it back.
Wrong. Millette did NOT say it.
He did NOT use extended sovent AND heat treatment. You make a FALSE statement there!

If you want to disagree, please support your claim with a quote from Millette's work!


You previously claimed that certain solvents ALONE are expected to dissolve epoxy. Do you retract that claim? If not, please provide a citation to support it!
 
To their credit, several 9/11 Truth activists agree with me that Jones/Harrit/Ryan should release samples of their chips to Millette. One of them even called Kevin Ryan's behavior "childish."

i also agree that they should release their chips to millette. i bet if anything ever happened, one member of jones and crew would like to be present when the chips are tested.
 

Back
Top Bottom